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10.2 hplc analysis 10.2.1 the hplc system is assembled and calibrated as described in section 11 Find methods for your needs analysis of phenol standards by epa method 604 be the first to rate this application compounds method system The operating parameters are as follows :
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A method for simultaneous determination of 11 phenols in drinking water was developed and validated The separated compounds are carried past an electrochemical detector with the flow of eluent through the system. The analytes were extracted by solid phase extraction (spe) with an agilent bond elut plexa cartridge, and separated by hplc using an agilent poroshell 120 column.
The analytical procedure presented in this method uses reverse phase hplc with ultraviolet (uv) detection at 218 nm, since the unresolved cresol isomers respond equally at this wavelength
An alternate gas chromatographic method using flame ionization detection is also quite satisfactory. Hplc methods for analysis of phenol. An aliquot of filtered sample is injected onto a liquid chromatography column, where it is separated by reverse phase hplc